Observed and calculated structure factors for biotite-1M crystals: A4
H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/
1 1 1 40.4 -40.9 -1 9 8 17.7 18.9 1 1 6 28.8 -29.5
1 1 0 28.4 31.7 -1 9 9 49.3 -48.9 1 1 4 10.0 9.8
-1 1 1 12.8 13.9 -1 9 11 13.3 -13.8 1 1 3 41.2 -40.6
-1 1 2 60.3 -63.6 1 11 0 19.3 20.6 1 1 2 79.8 -83.5
-1 1 3 77.1 -77.6 -1 11 2 26.4 -27.9 0 12 7 35.0 -37.3
-1 1 4 17.8 -17.2 -1 11 3 24.2 -25.0 0 12 4 39.8 41.4
-1 1 5 10.5 10.7 -1 11 5 18.3 18.0 0 12 3 34.1 -34.9
-1 1 7 37.3 -37.8 -1 11 7 20.1 -21.7 0 12 2 7.6 8.2
-1 1 8 15.7 -16.4 1 13 1 12.4 -11.5 0 12 1 26.8 -28.5
-1 1 11 17.2 -17.8 1 13 0 9.2 8.7 0 12 0 76.5 79.0
-1 1 12 12.8 -12.1 -1 13 3 13.9 -14.5 0 10 9 10.3 -9.9
-1 1 15 12.6 -11.5 1 13 4 11.4 11.1 0 10 7 16.8 16.6
1 3 1 9.0 9.1 1 13 2 17.9 -18.0 0 10 6 16.6 17.6
1 3 0 25.2 -22.5 1 11 6 10.1 -10.1 0 10 4 7.9 -7.7
-1 3 1 146.7 -146.0 1 11 3 14.3 -14.6 0 10 3 8.3 8.3
-1 3 2 122.0 122.0 1 11 2 18.4 -18.1 0 10 2 22.0 22.8
-1 3 3 130.7 -130.7 1 9 11 7.6 6.9 0 8 12 12.7 12.8
-1 3 4 73.4 73.3 1 9 10 24.6 25.9 0 8 11 18.2 18.2
-1 3 5 149.0 -148.5 1 9 9 42.7 -43.1 0 8 9 16.0 -16.0
-1 3 6 71.2 70.1 1 9 7 35.7 -36.2 0 8 7 26.7 27.2
-1 3 9 84.9 -82.7 1 9 6 70.4 72.8 0 8 6 29.9 31.3
-1 3 10 9.6 10.4 1 9 5 57.3 -57.6 0 8 4 11.8 -12.0
-1 3 11 10.1 -10.2 1 9 3 43.2 -43.6 0 8 2 27.4 26.1
-1 3 12 59.3 59.1 1 9 2 48.4 48.1 0 8 1 16.0 15.2
-1 3 13 62.7 -59.6 1 7 11 11.4 -12.3 0 6 13 10.9 8.0
-1 3 15 20.8 -18.7 1 7 10 17.0 -17.6 0 6 12 19.5 20.4
1 5 1 45.8 -43.4 1 7 6 12.1 -12.4 0 6 11 58.1 -56.1
1 5 0 21.3 20.1 1 7 3 24.9 -25.9 0 6 10 51.3 49.1
-1 5 1 19.5 19.3 1 7 2 35.2 -34.4 0 6 9 9.4 -10.4
-1 5 2 30.9 -30.5 1 5 11 13.5 -13.4 0 6 8 75.5 73.2
-1 5 3 45.3 -45.6 1 5 7 28.2 -28.7 0 6 7 70.2 -72.1
-1 5 4 16.4 -16.1 1 5 6 29.9 -30.9 0 6 6 11.6 11.9
-1 5 7 27.6 -27.8 1 5 5 8.5 8.6 0 6 5 20.8 18.5
-1 5 11 18.2 -18.6 1 5 4 21.7 22.7 0 6 4 88.3 87.4
-1 5 12 13.7 -12.3 1 5 3 19.2 -19.8 0 6 3 52.9 -53.7
1 7 0 28.1 28.3 1 5 2 60.0 -61.5 0 6 2 36.3 33.7
-1 7 2 49.1 -48.1 1 3 14 20.8 21.1 0 6 1 73.9 -74.0
-1 7 3 47.3 -47.4 1 3 13 50.8 -46.4 0 6 0 177.8 177.3
-1 7 5 22.0 23.6 1 3 12 12.5 12.6 0 4 12 21.7 19.0
-1 7 7 30.5 -31.3 1 3 10 25.5 24.9 0 4 11 26.3 26.2
-1 7 8 18.4 -18.7 1 3 9 77.2 -76.9 0 4 9 27.1 -27.4
1 9 1 28.3 -27.1 1 3 7 51.0 -48.9 0 4 8 10.8 -11.9
1 9 0 14.0 -13.4 1 3 6 143.8 143.0 0 4 7 42.5 42.4
-1 9 1 68.4 -65.0 1 3 5 123.9 -124.2 0 4 6 56.9 56.6
-1 9 2 84.1 82.7 1 3 4 13.3 -12.9 0 4 5 16.5 16.3
-1 9 3 38.5 -37.9 1 3 3 103.9 -103.4 0 4 4 22.4 -24.1
-1 9 4 21.4 22.2 1 3 2 69.8 68.8 0 4 3 14.6 -14.7
-1 9 5 94.4 -93.6 1 1 11 16.8 -15.5 0 4 2 28.2 29.2
-1 9 6 35.5 35.9 1 1 10 15.4 -15.9 0 4 1 41.4 41.1
-1 9 7 12.0 10.2 1 1 7 29.0 -28.4 0 4 0 47.9 46.5
1
H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/
0 2 15 13.5 12.7 -2 8 1 15.5 -15.8 -2 0 8 48.6 48.8
0 2 13 12.0 -10.0 2 6 12 54.7 52.3 -2 0 10 77.4 78.4
0 2 11 17.8 18.5 2 6 11 36.0 -38.0 -2 0 11 24.4 -24.5
0 2 10 12.5 12.2 2 6 10 14.2 15.3 -2 0 13 12.7 -12.9
0 2 7 34.9 34.7 2 6 9 16.6 -15.9 -2 0 14 48.3 46.2
0 2 6 21.0 21.3 2 6 8 49.3 48.5 -2 0 15 21.5 -21.1
0 2 5 11.9 -12.4 2 6 7 18.2 -18.2 -2 2 2 40.6 44.5
0 2 3 59.3 59.8 2 6 5 27.4 -27.9 -2 2 3 14.0 14.9
0 2 2 82.3 82.3 2 6 4 118.8 118.7 -2 2 4 22.7 -22.8
0 2 1 11.0 10.1 2 6 3 56.9 -58.8 -2 2 5 13.5 -14.8
0 2 0 43.5 -42.7 2 6 2 35.3 36.0 -2 2 6 29.9 31.5
0 0 15 33.1 -29.6 2 6 1 108.3 -103.3 -2 2 7 57.9 60.3
0 0 14 18.9 18.7 2 6 0 121.1 120.4 -2 2 8 25.6 27.3
0 0 13 15.3 15.1 -2 6 1 45.0 44.0 -2 2 9 25.6 -26.0
0 0 12 41.2 38.5 2 4 10 13.2 12.5 -2 2 10 17.1 -17.4
0 0 11 59.7 -59.8 2 4 7 16.8 17.7 -2 2 11 11.6 13.5
0 0 10 61.1 58.0 2 4 6 34.2 34.9 -2 2 12 27.7 29.2
0 0 9 40.3 -39.2 2 4 5 7.4 7.0 -2 2 13 11.8 10.6
0 0 8 83.8 83.2 2 4 4 19.2 -20.7 -2 4 2 11.8 12.6
0 0 7 80.1 -79.2 2 4 2 50.3 54.9 -2 4 3 47.1 47.8
0 0 6 59.9 60.3 2 4 1 49.6 52.9 -2 4 4 26.6 27.4
0 0 5 76.7 75.7 -2 4 1 27.0 -27.6 -2 4 7 19.9 20.8
0 0 4 77.7 76.7 2 2 11 27.2 25.7 -2 4 8 15.4 16.2
0 0 3 140.1 -140.2 2 2 10 22.1 22.2 -2 4 9 8.7 -8.6
0 0 2 19.6 20.3 2 2 8 28.6 -29.6 -2 4 11 15.7 17.4
0 0 1 87.8 -88.7 2 2 6 56.6 56.7 -2 4 12 15.2 15.7
0 12 6 10.6 11.0 2 2 5 44.6 46.5 -2 4 14 10.6 -10.8
1 1 13 9.3 9.1 2 2 3 25.1 -27.9 -2 6 2 26.0 24.4
1 7 7 8.6 -8.3 2 2 1 33.8 36.7 -2 6 3 91.6 -87.8
-1 11 8 10.2 -10.1 2 2 0 43.8 46.0 -2 6 4 42.1 39.2
-1 5 6 7.6 -8.1 -2 2 1 38.4 39.7 -2 6 6 104.5 101.6
2 12 5 20.8 -21.3 2 0 14 19.9 18.0 -2 6 7 79.7 -81.5
2 12 4 51.7 55.5 2 0 12 60.3 59.9 -2 6 8 39.1 39.7
2 12 3 24.4 -24.2 2 0 11 59.7 -58.8 -2 6 9 15.2 -15.7
2 12 2 18.1 18.5 2 0 10 12.1 11.4 -2 6 10 45.9 46.5
2 12 1 46.0 -48.1 2 0 9 10.5 -10.7 -2 6 11 23.5 -24.6
2 12 0 51.2 50.9 2 0 8 82.5 81.8 -2 8 2 14.4 14.5
-2 12 1 11.6 9.7 2 0 5 67.7 -69.2 -2 8 3 25.2 25.4
2 10 8 12.7 -11.0 2 0 4 150.1 149.7 -2 8 4 12.1 10.7
2 10 6 20.3 22.7 2 0 3 71.3 -72.5 -2 8 7 20.7 21.7
2 10 5 12.1 11.4 2 0 2 130.6 132.0 -2 8 8 11.4 12.4
2 10 3 10.0 -9.5 2 0 1 126.3 -124.9 -2 8 11 10.5 9.6
2 10 2 15.1 14.6 2 0 0 145.9 145.6 -2 8 12 14.7 15.4
2 10 1 18.5 17.9 -2 0 1 22.9 20.7 -2 10 2 12.0 10.7
2 8 11 12.4 11.3 -2 0 2 9.5 -8.6 -2 10 3 14.3 14.7
2 8 10 10.7 10.3 -2 0 3 66.3 -67.2 -2 10 5 7.9 -7.7
2 8 6 25.2 28.1 -2 0 4 106.2 104.3 -2 10 6 8.6 8.1
2 8 4 15.0 -14.7 -2 0 5 16.9 14.3 -2 10 7 18.0 18.6
2 8 2 26.0 25.7 -2 0 6 124.5 124.9 -2 10 8 10.8 10.3
2 8 1 29.8 30.2 -2 0 7 141.6 -144.3 -2 10 9 12.0 -11.2
1
H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/
-2 12 2 11.9 12.1 3 9 9 37.7 -38.8 4 10 5 13.5 13.7
-2 12 3 45.8 -43.2 -3 11 1 12.0 11.6 4 10 3 11.8 -11.7
-2 12 4 24.7 24.8 3 11 1 21.2 -21.1 4 10 1 17.1 18.5
-2 12 6 44.2 45.4 3 11 2 9.5 -9.0 4 10 0 12.9 12.4
-2 12 7 46.2 -46.8 3 11 5 11.8 -11.6 4 8 7 8.4 -8.3
-3 1 1 21.9 24.3 3 11 6 12.3 -14.7 4 8 6 13.5 13.7
3 1 1 38.2 -41.7 -3 13 1 9.7 9.4 4 8 5 22.9 24.3
3 1 2 37.0 -39.2 -3 11 8 11.5 -11.2 4 8 3 15.0 -13.9
3 1 5 16.2 -17.7 -3 11 3 17.3 -16.5 4 8 1 17.9 18.6
3 1 6 20.9 -21.4 -3 9 11 26.1 -27.4 4 8 0 19.5 18.4
3 1 9 12.1 -13.8 -3 9 9 55.2 -54.6 4 6 9 26.2 -26.2
3 1 10 17.1 -18.6 -3 9 8 41.7 40.6 4 6 8 44.3 43.1
3 1 12 11.6 10.4 -3 9 5 47.4 -47.1 4 6 6 37.1 37.2
-3 3 1 187.8 -180.3 -3 9 4 30.6 31.9 4 6 5 70.3 -74.3
3 3 0 75.1 75.2 -3 9 3 27.0 -27.2 4 6 4 56.8 60.1
3 3 1 34.8 -34.2 -3 9 2 33.2 31.1 4 6 3 10.3 -7.3
3 3 2 48.2 53.0 -3 7 12 13.1 -13.2 4 6 2 45.1 44.5
3 3 3 88.1 -88.1 -3 7 8 15.2 -17.2 4 6 1 49.3 -49.7
3 3 4 19.0 -18.1 -3 7 7 17.3 -17.2 4 6 0 27.3 27.1
3 3 5 11.6 -11.0 -3 7 4 17.1 -15.1 -4 6 1 17.5 14.4
3 3 6 72.3 73.4 -3 7 3 26.6 -27.5 4 4 10 16.2 17.0
3 3 7 72.1 -75.5 -3 5 8 32.3 -33.7 4 4 9 10.7 10.6
3 3 9 49.0 -49.9 -3 5 7 14.7 -15.5 4 4 8 12.4 -11.9
3 3 10 58.2 57.6 -3 5 6 23.3 24.2 4 4 7 13.1 -13.7
3 3 11 18.8 -19.8 -3 5 5 14.2 15.4 4 4 6 18.7 17.4
-3 5 1 26.5 27.6 -3 5 4 28.0 -29.1 4 4 5 32.6 33.3
3 5 0 12.2 11.6 -3 5 3 59.0 -59.7 4 4 4 11.3 12.9
3 5 1 28.3 -29.0 -3 5 2 17.1 -17.7 4 4 3 14.1 -14.5
3 5 2 32.8 -32.6 -3 3 13 20.5 -20.9 4 4 1 20.2 21.4
3 5 3 9.4 -9.3 -3 3 12 57.0 57.4 4 4 0 20.8 20.9
3 5 5 11.5 -12.6 -3 3 11 51.5 -50.0 4 2 6 25.7 27.1
3 5 6 12.5 -13.2 -3 3 9 72.9 -74.4 4 2 5 24.5 25.9
3 5 9 13.8 -13.7 -3 3 8 71.3 72.6 4 2 3 22.9 -26.0
3 5 10 16.6 -17.5 -3 3 7 13.3 -12.1 4 2 2 15.0 14.3
3 5 12 12.3 12.2 -3 3 6 19.2 -19.2 4 2 1 55.0 55.3
-3 7 1 10.4 10.7 -3 3 5 89.3 -88.7 4 2 0 34.4 37.0
3 7 0 11.1 -8.9 -3 3 4 55.9 55.1 -4 2 1 15.7 -17.2
3 7 1 33.8 -33.7 -3 3 3 36.6 -35.1 4 0 9 25.8 -25.5
3 7 2 15.3 -16.8 -3 3 2 77.7 75.5 4 0 8 46.1 46.0
3 7 3 11.3 11.4 -3 1 12 11.4 -12.2 4 0 7 13.8 -15.2
3 7 5 18.0 -17.0 -3 1 8 33.7 -36.0 4 0 6 39.9 41.5
3 7 6 21.4 -22.0 -3 1 7 19.5 -20.3 4 0 5 84.3 -83.5
3 7 10 12.9 -10.9 -3 1 6 17.0 17.5 4 0 4 102.0 103.2
-3 9 1 91.6 -89.3 -3 1 5 12.7 12.7 4 0 2 38.7 40.7
3 9 0 55.7 52.1 -3 1 4 32.5 -34.5 4 0 1 86.6 -88.8
3 9 2 30.7 29.9 -3 1 3 64.9 -67.5 4 0 0 23.8 24.3
3 9 3 65.6 -66.0 -3 1 2 16.4 -17.7 -4 0 1 47.6 45.6
3 9 4 12.8 -11.9 -3 1 13 8.2 -8.3 -4 0 2 121.0 121.9
3 9 6 54.2 56.4 4 12 0 14.3 14.9 -4 0 3 104.4 -104.5
3 9 7 38.5 -43.1 4 10 6 11.1 11.2 -4 0 4 35.4 36.9
1
H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/
-4 0 5 58.1 -60.4 -5 3 1 71.6 -68.6 -5 1 13 12.8 -12.9
-4 0 6 122.1 122.5 5 3 0 91.1 87.1 -5 1 9 20.0 -19.6
-4 0 7 29.5 -29.0 5 3 1 40.0 -39.8 -5 1 8 22.8 -23.8
-4 0 9 18.0 -18.7 5 3 2 22.6 23.5 -5 1 6 14.3 14.2
-4 0 10 49.3 50.0 5 3 3 98.8 -97.2 -5 1 4 32.7 -33.5
-4 0 11 15.5 -15.2 5 3 4 39.2 36.8 -5 1 3 22.1 -21.8
-4 0 12 13.4 15.3 5 3 5 11.7 11.3 -5 1 2 10.6 10.5
-4 0 13 36.4 -38.8 5 3 6 18.7 19.1 6 8 3 9.9 -9.9
-4 0 14 52.3 53.2 5 3 7 49.9 -50.1 6 8 1 11.5 10.8
-4 2 2 22.5 -25.1 5 3 9 14.3 -14.9 6 8 0 21.9 20.6
-4 2 3 15.9 18.6 5 5 0 21.7 -20.7 6 6 5 36.9 -39.4
-4 2 4 37.1 38.7 5 5 1 17.6 -18.3 6 6 4 12.3 10.9
-4 2 5 17.1 16.7 5 5 4 14.4 -11.2 6 6 2 43.9 43.4
-4 2 8 16.7 17.9 5 5 5 20.9 -22.1 6 6 1 37.2 -35.8
-4 2 11 9.8 9.9 5 5 7 12.8 10.4 -6 6 1 30.5 -30.8
-4 2 12 16.5 18.3 -5 7 1 13.4 12.4 6 4 5 19.2 19.2
-4 2 13 8.9 8.8 5 7 1 22.5 -21.2 6 4 4 9.0 8.9
-4 4 2 8.0 8.2 -5 9 1 54.8 -52.3 6 4 3 13.1 -13.1
-4 4 3 24.1 24.8 5 9 0 53.0 50.1 6 4 2 11.7 -12.6
-4 4 4 14.2 15.3 5 9 1 18.8 -20.1 6 4 1 18.0 17.7
-4 4 5 11.6 -13.2 5 9 2 25.3 24.4 6 4 0 30.9 31.3
-4 4 7 18.6 20.2 5 9 3 59.0 -57.5 -6 4 1 10.9 8.3
-4 4 8 33.4 34.8 5 9 4 23.3 22.7 6 2 5 15.5 17.4
-4 4 10 15.6 -17.1 -5 11 2 12.6 10.5 6 2 4 19.2 18.8
-4 4 12 13.9 15.2 -5 9 8 49.6 48.5 6 2 1 7.9 7.9
-4 4 13 14.9 15.4 -5 9 7 47.7 -47.1 6 2 0 17.4 17.7
-4 6 2 70.4 66.9 -5 9 5 26.1 -25.6 6 0 8 29.3 29.3
-4 6 3 88.0 -84.4 -5 9 4 44.9 44.2 6 0 6 59.0 57.1
-4 6 4 39.3 38.9 -5 9 3 15.4 -12.5 6 0 5 44.0 -43.5
-4 6 5 22.9 -23.1 -5 7 9 17.7 -18.2 6 0 2 49.3 49.5
-4 6 6 95.6 96.6 -5 7 8 15.2 -14.3 6 0 1 31.6 -32.0
-4 6 7 34.6 -37.0 -5 7 6 17.5 16.4 6 0 0 27.5 26.8
-4 6 8 12.1 -10.5 -5 7 4 31.5 -30.6 -6 0 1 35.8 -34.0
-4 6 9 19.7 -19.4 -5 7 3 20.1 -20.0 -6 0 2 93.7 93.8
-4 6 10 47.6 50.3 -5 7 2 11.4 11.4 -6 0 3 54.2 -54.0
-4 6 12 14.5 14.3 -5 5 10 10.2 10.1 -6 0 4 10.1 9.4
-4 8 3 15.5 16.2 -5 5 9 14.3 -13.8 -6 0 5 32.1 -31.9
-4 8 4 12.3 13.0 -5 5 8 23.8 -22.1 -6 0 6 73.5 68.8
-4 8 8 22.8 23.4 -5 5 6 9.8 9.7 -6 0 7 15.3 12.6
-4 8 10 11.8 -10.6 -5 5 4 21.9 -22.1 -6 0 9 56.3 -58.2
-4 10 3 11.6 10.4 -5 5 3 16.4 -15.3 -6 0 10 42.0 45.2
-4 10 4 15.7 14.5 -5 3 12 27.8 26.7 -6 0 12 39.1 41.2
-4 12 2 37.5 38.4 -5 3 11 45.7 -45.2 -6 2 3 8.7 8.7
-4 12 3 45.3 -45.0 -5 3 9 37.2 -37.9 -6 2 4 23.4 24.7
5 1 0 18.1 -19.9 -5 3 8 77.4 75.2 -6 2 6 11.0 -11.2
5 1 1 24.9 -25.5 -5 3 7 62.7 -61.3 -6 2 8 20.2 19.5
5 1 4 11.0 -11.7 -5 3 5 46.3 -43.9 -6 2 9 21.6 22.3
5 1 5 19.1 -20.6 -5 3 4 51.7 50.2 -6 2 11 12.2 -11.8
5 1 9 14.4 -14.4 -5 3 3 29.6 -28.3 -6 4 2 15.0 -15.8
5 1 10 9.5 -9.9 -5 3 2 18.1 -14.8 -6 4 4 19.3 19.3
1
H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/
-6 4 5 16.9 16.7 7 3 0 47.3 45.3 -7 3 4 53.7 51.8
-6 6 2 86.3 84.0 7 3 1 27.1 -27.5 -7 3 3 51.5 -53.9
-6 6 3 31.8 -30.5 7 3 3 47.3 -48.6 -7 3 2 11.8 -10.9
-6 6 4 11.1 9.7 7 3 4 47.0 51.4 -7 1 9 16.6 -18.7
-6 6 5 36.6 -37.0 7 5 0 13.1 -15.0 -7 1 5 15.5 -17.0
-6 6 6 43.9 43.8 -7 5 7 10.8 10.8 -7 1 4 17.4 -18.9
-6 6 8 12.0 11.2 -7 5 5 17.1 -17.4 -7 1 7 8.8 8.7
-6 6 9 37.1 -39.0 -7 5 4 17.3 -18.6 -8 0 1 47.1 -49.5
-6 8 2 11.9 -12.9 -7 5 2 12.5 11.9 -8 0 2 44.5 42.2
-6 8 4 13.8 15.2 -7 3 8 22.5 23.3 -8 0 3 15.9 7.9
-6 8 5 10.3 10.4 -7 3 7 57.1 -61.4 -8 0 4 18.9 16.3
7 1 0 17.1 -16.7 -7 3 6 25.6 25.9 -8 0 5 35.1 -35.5
7 1 4 12.1 -13.3 -7 3 5 21.3 -20.4 -8 2 3 13.9 -14.1
-7 3 1 15.0 -12.6